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Evaporation & Rectification

Evaporation & Rectification – concept and selection

corosys builds evaporator systems for a wide range of applications in the beverage, food and chemical-pharmaceutical industries. For this purpose, we have built up and continuously developed special know-how, notably for film evaporation applications. Central differences between film evaporators and conventional evaporators are the very short retention time and the negligible hydrostatic pressure on the boiling liquid, which allows operation at very low pressures and thus significantly reduced boiling temperatures. Accordingly, these evaporator systems are particularly suitable for the evaporation of high-boiling and temperature-sensitive mixtures of substances.

Evaporator type Lab & Pilot Production Visc. Foam Fouling Solids CIP T-sensitiv VWZ Retention Time
Falling Film EFF 0,06 – 1,5 m² bis >1.000 m² - + o o + +/o + +
Thin Film ETF 0,02 – 0,6 m² bis >10 m² + + + + o + + o
Short Film ESF 0,02 – 0,3 m² bis >10 m² + - + + o ++ + -

1) Laboratory & pilot plants are offered as standardized systems, production plants are designed on request
2) Selection criteria are listed as examples, further process-dependent criteria will be considered in cooperation with our customers

Combinations are advantageous for many applications:

  • Combinations of evaporators with each other – e.g. for the evaporation of larger quantities of solvent in a falling film evaporator stage and downstream a concentration of the remaining higher boiling components in e.g. a thin film or short path evaporator stage.
  • Combinations of evaporators with a separation column – e.g. for the separation of higher boiling mixtures with closely spaced boiling points of the components to be separated.

Some of the standard combinations are shown in the following table. In addition, further process-specific variants are considered and implemented in cooperation with the customer.

Verdampfertypen Typische Anwendung
Verdampferkombination EFF-ETF Ausgangsgemisch mit Schwersieder und großer Menge niederviskoser Leichtsieder
Verdampferkombination EFF-ESF Ausgangsgemisch mit sehr hoch siedenden Schwersiedern und großer Menge niederviskoser Leichtsieder
Fallfilmverdampfer mit Rektifikation EFR Ausgangsgemisch mit mit eng beieinander liegenden Siedepunkten der Komponenten
Dünnschichtverdampfer mit Rektifikation  ETR Ausgangsgemisch mit eng beieinander liegenden Siedepunkten der Komponenten und hochsiedender  Teilfraktion

In addition to known processes, this method can only be used to pre-select the appropriate unit or combination of units and to make a rough estimate of the sizes and costs. For validation, tests are then required for most applications. For these validation tests different corosys evaporator types are available, which can be carried out by corosys or at the customer’s site with corosys support, depending on the customer and application. To characterize the separation task, please use the attached evaporator form or contact our experts directly.

Known and newly developed processes alike will gladly be evaluated beyond that. If desired, together with our customers, we check for possibilities of energy saving as well as resource-saving plant cleaning within the scope of our engineering. Especially for processes with a relevant and largely homogeneous low-boiling component, numerous applications have been developed in recent years. Examples are given in the section “Applications”.